|
鍙嬫儏鎻愮ず锛氭湰绔欐彁渚涘叏鍦�400澶氭墍楂樼瓑闄㈡牎鎷涙敹纰╁＋銆佸崥澹爺绌剁敓鍏ュ(xu茅)鑰冭│姝峰勾鑰冪爺鐪熼銆佽€冨崥鐪熼銆佺瓟妗�锛岄儴鍒嗗(xu茅)鏍℃洿鏂拌嚦2012骞�锛�2013骞达紱鍧囨彁渚涙敹璨�(f猫i)涓嬭級銆� 涓嬭級娴佺▼锛� 鑰冪爺鐪熼 榛�(di菐n)鎿娾€�鑰冪爺瑭﹀嵎鈥濃€濅笅杓�; 鑰冨崥鐪熼 榛�(di菐n)鎿娾€�鑰冨崥瑭﹀嵎搴�鈥� 涓嬭級
1
鑿腑绉戞妧澶у(xu茅)纰╁＋鐮旂┒鐢熷叆瀛�(xu茅)鑰冭│銆婃湁姗�(j墨)鍖栧(xu茅)銆嬭€冭│澶х侗
锛堝皥妤�(y猫)浠ｇ⒓锛�874锛�
绗竴閮ㄥ垎 鑰冭│瑾槑
涓€銆佽€冭│鎬ц唱(zh矛)
鍏ㄥ湅纰╁＋鐮旂┒鐢熷叆瀛�(xu茅)鑰冭│鏄偤楂樼瓑瀛�(xu茅)鏍℃嫑鏀剁ⅸ澹爺绌剁敓鑰岃ō(sh猫)缃殑銆傚叾涓�锛屾湁姗�(j墨)鍖栧(xu茅)灞垜
鏍￠€�(j矛n)琛屽懡椤岀殑鑰冭│绉戠洰銆傚畠鐨勮⿻鍍�(ji脿)妯�(bi膩o)婧�(zh菙n)鏄細楂樼瓑瀛�(xu茅)鏍″劒(y艒u)绉€鐣㈡キ(y猫)鐢熻兘閬�(d谩)鍒板強鏍兼垨鍙婃牸浠ヤ笂姘村钩锛�
浠ヤ繚璀夎閷勫彇鑰呭叿鏈夎純鎵庡(sh铆)鐨勬湁姗�(j墨)鍖栧(xu茅)鍩虹(ch菙)鐭ヨ瓨(sh铆)銆�
浜�銆佽€冭│鐨勮寖鍦�
鑰冭│鑼冨湇鍖呮嫭鏈夋(j墨)鍖栧(xu茅)鐨勭祼(ji茅)妲�(g貌u)銆佸懡鍚�銆佺暟妲�(g貌u)鐝�(xi脿n)璞�銆佸厜璀滄暩(sh霉)鎿�(j霉)瑙ｆ瀽銆佸悇椤炴湁姗�(j墨)鍖栧悎鐗╃殑鐗�
鐞嗘€ц唱(zh矛)鑸囧寲瀛�(xu茅)鎬ц唱(zh矛)?锛熺柧姗愵仜c(di菐n)瑭宠鏈侗绗簩閮ㄥ垎銆�
涓夈€佽⿻鍍�(ji脿)鐩(bi膩o)
鏈夋(j墨)鍖栧(xu茅)鑰冭│鍦ㄨ€冩煡鍩烘湰鐭ヨ瓨(sh铆)銆佸熀鏈悊璜栫殑鍩虹(ch菙)涓婏紝娉ㄩ噸鑰冩煡鑰冪敓闈堟椿閬�(y霉n)鐢ㄩ€欎簺鍩虹(ch菙)鐭�
璀�(sh铆)瑙€瀵熷拰瑙ｆ焙瀵�(sh铆)闅涘晱椤岀殑鑳藉姏銆傝€冪敓鎳�(y墨ng)鑳斤細
1锛庢纰烘帉鎻″拰鐞嗚В鍚勬湁姗�(j墨)鍖栧悎鐗╃殑绲�(ji茅)妲�(g貌u)銆佸懡鍚嶆柟娉曪紱
2锛庣啛绶存帉鎻″熀绀�(ch菙)鏈夋(j墨)鍖栧(xu茅)鍙嶆噳(y墨ng)鐨勫師鐞嗗強鎳�(y墨ng)鐢ㄨ寖鍦�锛�
3锛庣啛绶存帉鎻℃湁姗�(j墨)鍖栧(xu茅)鍙嶆噳(y墨ng)鐨勫熀鏈悊璜�銆佸熀鏈蹇典互鍙婂弽鎳�(y墨ng)姗�(j墨)鐞嗙瓑锛岀壒鍒ユ敞鎰忕悊瑙ｅ拰鎺�
鎻℃湁姗�(j墨)鍖栧(xu茅)鍙嶆噳(y墨ng)涓殑绔嬮珨鍖栧(xu茅)鍟忛锛�
4锛庣啛鎮夊悇椤為噸瑕佹湁姗�(j墨)鍚堟垚鍖栧(xu茅)鍙嶆噳(y墨ng)銆佷簡瑙ｆ湁姗�(j墨)鍚堟垚鐨勫熀鏈蹇靛拰鐭ヨ瓨(sh铆)銆�
5锛庢纰烘帉鎻℃湁姗�(j墨)鍖栧悎鐗╃殑绲�(ji茅)妲�(g貌u)瑙ｆ瀽鏂规硶銆�
6锛庢帉鎻℃湁姗�(j墨)鍖栧(xu茅)瀵�(sh铆)椹�(y脿n)鐨勫熀鏈煡璀�(sh铆)鍜屾妧鑳姐€�
鍥�銆佽€冪敓褰㈠紡鑸囪│鍗风祼(ji茅)妲�(g貌u)
锛堜竴锛夌瓟鍗锋柟寮忥細闁夊嵎锛岀瓎瑭�銆�
锛堜簩锛夌瓟椤屾檪(sh铆)闁擄細180 鍒嗛悩銆�
锛堜笁锛夊悇閮ㄥ垎鍏�(n猫i)瀹圭殑鑰冩煡姣斾緥
瑭﹀嵎婊垮垎鐐� 150 鍒�銆�
鍩虹(ch菙)鐭ヨ瓨(sh铆)锛堝熀鏈蹇�銆佸熀鏈悊璜栥€佸熀鏈弽鎳�(y墨ng)锛夌磩 55%
鏈夋(j墨)鍚堟垚 绱� 20%
姗�(j墨)鐞嗛 绱� 10%
鎺ㄦ柗绲�(ji茅)妲�(g貌u)锛堝惈娉㈣瓬鍒嗘瀽锛夌磩 10%
瀵�(sh铆)椹�(y脿n) 绱� 5锛�
绗簩閮ㄥ垎 鑰冩煡瑕侀粸(di菐n)
绗竴绔� 绶掕珫
1.鏈夋(j墨)鍖栧(xu茅)鍜屾湁姗�(j墨)鍖栧悎鐗�
2.鍏卞児(ji脿)閸电殑鍩烘湰鎬ц唱(zh矛)
3.鐮旂┒鏈夋(j墨)鍖栧悎鐗╃殑鍩烘湰鏂规硶
4.鏈夋(j墨)鍖栧悎鐗╃殑鍒嗛
绗簩绔� 鐑风兇
2
1.鐑风兇鐨勭暟妲�(g貌u)鑸囧懡鍚�
2.鐑风兇鐨勬(g貌u)鍨嬭垏妲�(g貌u)璞�
3.鐑风兇鐨勭墿鐞嗘€ц唱(zh矛)
4.鐑风兇鐨勫寲瀛�(xu茅)鎬ц唱(zh矛)
5.楣典唬鍙嶆噳(y墨ng)鐨勬(j墨)鐞�锛岃嚜鐢卞熀鐨勭┅(w臎n)瀹氭€�
绗笁绔� 鐠�(hu谩n)鐑风兇
1.鐠�(hu谩n)鐑风兇鐨勫懡鍚嶈垏鐣版(g貌u)
2.鐠�(hu谩n)鐑风兇鐨勭墿鐞嗚垏鍖栧(xu茅)鎬ц唱(zh矛)
3.鐠�(hu谩n)鐑风兇鐨勬(g貌u)璞″強妲�(g貌u)璞″垎鏋�
4.澶氱挵(hu谩n)鐑�
绗洓绔� 灏嶆槧鐣版(g貌u)
1.鏃嬪厜鎬�
2.鎵嬫€�
3.鍒嗗瓙鐨勬墜鎬ц垏灏嶇ū鎬�
4.鍚竴鍊�(g猫)鎵嬫€х⒊鍘熷瓙鐨勫寲鍚堢墿
5.鍚咕鍊�(g猫)鎵嬫€х⒊鍘熷瓙鐨勯枊閺堝寲鍚堢墿
6.纰崇挵(hu谩n)鍖栧悎鐗╃殑绔嬮珨鐣版(g貌u)
绗簲绔� 楣典唬鐑�
锛戯紟楣典唬鐑风殑鍛藉悕
锛掞紟楣典唬鐑风殑绲�(ji茅)妲�(g貌u)鍜岀墿鐞嗘€ц唱(zh矛)
锛擄紟楣典唬鐑风殑鍖栧(xu茅)鎬ц唱(zh矛)
锛旓紟瑕牳鍙栦唬鍙嶆噳(y墨ng)姗�(j墨)鐞�
锛曪紟楣典唬鐑风殑鍒舵硶
锛栵紟鏈夋(j墨)閲戝爆鍖栧悎鐗�
绗叚绔� 鐑兇
锛戯紟鐑兇鐨勭祼(ji茅)妲�(g貌u)銆佺暟妲�(g貌u)鍜屽懡鍚�
锛掞紟鐑兇鐨勫埗娉�
锛擄紟娑堝幓鍙嶆噳(y墨ng)姗�(j墨)鐞�
锛旓紟鐑兇鐨勭墿鐞嗘€ц唱(zh矛)
锛曪紟鐑兇鐨勫寲瀛�(xu茅)鎬ц唱(zh矛)
锛栵紟瑕浕鍔犳垚鍙嶆噳(y墨ng)姗�(j墨)鐞�锛岀⒊姝ｉ洟瀛愮殑绌�(w臎n)瀹氭€�
锛楋紟鐑兇鐨勪締婧愬拰鐢ㄩ€�
绗竷绔� 鐐旂兇鍜屼簩鐑兇
1. 鐐旂兇鐨勭祼(ji茅)妲�(g貌u)銆佺暟妲�(g貌u)鍜岀墿鐞嗘€ц唱(zh矛)
2. 鐐旂兇鐨勫寲瀛�(xu茅)鍙嶆噳(y墨ng)
3. 鐐旂兇鐨勫埗娉�
4. 鍏辫粵浣滅敤锛岃秴鍏辫粵浣滅敤
5. 鍏辫粵浜岀儻鐑�
6. 绱⿳浜岀儻鐑�
绗叓绔� 鑺崇兇
1. 鑻殑绲�(ji茅)妲�(g貌u)銆佸叡鎸珫
2. 鑻鐢熺墿鐨勭暟妲�(g貌u)銆佸懡鍚嶅強鐗╃悊鎬ц唱(zh矛)
3. 鑻挵(hu谩n)涓婄殑瑕浕鍙栦唬鍙嶆噳(y墨ng)鍙婃(j墨)鐞�
4. 鑻挵(hu谩n)涓婅Κ闆诲彇浠ｅ弽鎳�(y墨ng)鐨勫畾浣嶈(gu墨)寰�
3
5. 澶氱挵(hu谩n)鑺崇兇
6. 楣典唬鑺崇兇
7. 浼戝厠鐖捐(gu墨)寰�
绗節绔� 閱囥€侀厷銆侀啔
1. 閱囩殑绲�(ji茅)妲�(g貌u)銆佸懡鍚嶅拰鐗╃悊鎬ц唱(zh矛)
2. 涓€鍏冮唶鐨勫弽鎳�(y墨ng)
3. 涓€鍏冮唶鐨勫埗娉�
4. 浜屽厓閱�
5. 閰氱殑绲�(ji茅)妲�(g貌u)銆佸懡鍚嶅拰鐗╃悊鎬ц唱(zh矛)
6. 涓€鍏冮厷鐨勫弽鎳�(y墨ng)
7. 浜屽厓閰氬拰澶氬厓閰�
8. 閱氱殑绲�(ji茅)妲�(g貌u)銆佸懡鍚嶅拰鐗╃悊鎬ц唱(zh矛)
9. 閱氱殑鍙嶆噳(y墨ng)
10. 閱氱殑鍒舵硶
11. 鐠�(hu谩n)閱�
绗崄绔� 閱涖€侀叜銆侀唽
1. 涓€鍏冮啗閰殑绲�(ji茅)妲�(g貌u)銆佸懡鍚嶅拰鐗╃悊鎬ц唱(zh矛)
2. 閱涢叜鐨勮Κ鏍稿姞鎴愬弽鎳�(y墨ng)
3. 閱涢叜鐨勮Κ鏍稿姞鎴愬弽鎳�(y墨ng)姗�(j墨)鐞�
4. 閱涢叜鐨勬哀鍖栧拰閭勫師
5. 涓€鍏冮啗閰殑鍒舵硶
6. 閱涢叜鐨勪締婧愬拰鐢ㄩ€�
7. ?,?-涓嶉＝鍜岄啗閰�
8. 閱�
绗崄涓€绔犵晶閰�
1. 涓€鍏冪晶閰哥殑绲�(ji茅)妲�(g貌u)銆佸懡鍚嶅拰鐗╃悊鎬ц唱(zh矛)
2. 涓€鍏冪晶閰哥殑鍙嶆噳(y墨ng)
3. 涓€鍏冪晶閰哥殑鍒舵硶
4. 浜屽厓缇ч吀
绗崄浜岀珷缇ч吀琛嶇敓鐗�
1. 缇ч吀琛嶇敓鐗╃殑绲�(ji茅)妲�(g貌u)鍜屽懡鍚�
2. 缇ч吀琛嶇敓鐗╃殑鐗╃悊鎬ц唱(zh矛)
3. 閰按瑙ｅ弽鎳�(y墨ng)姗�(j墨)鐞�
4. 缇ч吀琛嶇敓鐗╃殑鍙嶆噳(y墨ng)
5. 缇ч吀琛嶇敓鐗╃殑鐢ㄩ€�
6. 鐑叜
7. 涓嶉＝鍜岀晶閰�
8. 鍙栦唬缇ч吀
9. 涔欓叞涔欓吀涔欓叝鍜屼笝浜岄吀浜屼箼閰強鍏跺湪鏈夋(j墨)鍚堟垚涓殑鎳�(y墨ng)鐢�
绗崄涓夌珷鍚爱鍖栧悎鐗�
1. 纭濆熀鍖栧悎鐗╃殑绲�(ji茅)妲�(g貌u)鍜屽懡鍚�
2. 纭濆熀鍖栧悎鐗╃殑鎬ц唱(zh矛)
3. 纭濆熀鍖栧悎鐗╃殑鍒跺倷
4. 鑳虹殑绲�(ji茅)妲�(g貌u)銆佸懡鍚嶅拰鐗╃悊鎬ц唱(zh矛)
4
5. 鑳虹殑鍖栧(xu茅)鎬ц唱(zh矛)
6. 鑳虹殑鍒舵硶
7. 鑺抽鏃忛噸姘寲鍙嶆噳(y墨ng)
8. 鑺抽鏃忛噸姘菇鐨勬€ц唱(zh矛)
9. 鍒嗗瓙閲嶆帓
绗崄鍥涚珷鏈夋(j墨)纭�銆佺７鍜岀鍖栧悎鐗�
1. 鍚～鍖栧悎鐗�
2. 鍚７鍖栧悎鐗�
3. 鍚鍖栧悎鐗�
绗崄浜旂珷闆滅挵(hu谩n)鍖栧悎鐗�
1. 闆滅挵(hu谩n)鍖栧悎鐗╃殑鍒嗛鍜屽懡鍚�
2. 浜斿厓闆滅挵(hu谩n)鍖栧悎鐗�
3. 鍏厓闆滅挵(hu谩n)鍖栧悎鐗�
4. 鐢熺墿鍫�
绗崄鍏珷鍛ㄧ挵(hu谩n)鍙嶆噳(y墨ng)
1. 鍛ㄧ挵(hu谩n)鍙嶆噳(y墨ng)鐞嗚珫
2. 闆荤挵(hu谩n)鍖栧弽鎳�(y墨ng)
3. 鐠�(hu谩n)鍔犳垚鍙嶆噳(y墨ng)
4. ?-閬风Щ鍙嶆噳(y墨ng)
绗崄涓冪珷纰虫按鍖栧悎鐗�
1. 鍠硸
2. 闆欑硸
3. 澶氱硸
4. 绯栫殑琛嶇敓鐗�
绗崄鍏珷鏈夋(j墨)鍚堟垚
锛戯紟 閫嗗悎鎴愬垎鏋�
锛掞紟 鏈夋(j墨)鍚堟垚瑷�(sh猫)瑷�(j矛)
绗崄涔濈珷 鏈夋(j墨)娉㈣瓬鍒嗘瀽锛圲V銆両R銆�
1
H NMR 鍜� MS 绛夛級
绗簩鍗佺珷 铔嬬櫧璩�(zh矛)銆佹皑鍩洪吀鍜屾牳閰�
绗簩鍗佷竴绔� 鏈夋(j墨)鍖栧(xu茅)瀵�(sh铆)椹�(y脿n)锛堝熀鏈師鐞�銆佸熀鏈搷浣滃拰鍩烘湰鍚堟垚鏂规硶锛�
鍏嶈铂(z茅)鑱叉槑锛氭湰鏂囩郴杞�(zhu菐n)杓夎嚜缍�(w菐ng)绲�(lu貌)锛屽鏈変镜鐘�锛岃珛鑱�(li谩n)绯绘垜鍊戠珛鍗冲埅闄わ紝鍙︼細鏈枃鍍呬唬琛ㄤ綔鑰呭€�(g猫)浜鸿榛�(di菐n)锛岃垏鏈恫(w菐ng)绔欑劇闂�(gu膩n)銆傚叾鍘熷壍(chu脿ng)鎬т互鍙婃枃涓櫝杩版枃瀛楀拰鍏�(n猫i)瀹规湭缍�(j墨ng)鏈珯璀夊(sh铆)锛屽皪鏈枃浠ュ強鍏朵腑鍏ㄩ儴鎴栬€呴儴鍒嗗収(n猫i)瀹�銆佹枃瀛楃殑鐪熷(sh铆)鎬�銆佸畬鏁存€с€佸強鏅�(sh铆)鎬ф湰绔欎笉浣滀换浣曚繚璀夋垨鎵胯锛岃珛璁€鑰呭儏浣滃弮鑰�锛屽苟璜嬭嚜琛屾牳瀵�(sh铆)鐩搁棞(gu膩n)鍏�(n猫i)瀹广€�
|
鏂囩珷鎼滅储
鎮ㄧ従(xi脿n)鍦ㄧ殑浣嶇疆锛� 
